To be clear:
On 07.01.2013, at 11:43, "Edward d'Auvergne" <edward.dauvergne@xxxxxxxxx>
wrote:
One strategy to overcome this was to
* record a HSQC/TROSY at different temperatures at the different
spectrometers
(conveniently by using Brukers multi_zgvt),
Did you use the trosy experiment for relaxation measurements?
I did not use *these* TROSYs for relaxation experiments, I recorded them
specifically to sort out the temperature problem. But I have TROSY-type
experiments from my relaxation measurements, of course the measurement
sequences are TROSY-based themselves, but I also record TROSYs in between
the (pseudo-)3Ds and at the end.
Cheers
Martin
Re: Temperature calibration: methanol- vs protein-based,